1、蘭州理工大學碩士學位論文NiO納米線和ATO納米粉的制備及表征姓名：馮耀華申請學位級別：碩士專業(yè)：有色金屬冶金指導教師：朱福良20080502NiO納米線和A1rO納米粉的制備及表征AbstractNiONano。powdershaVebeenusedinsuchareasascatalyst，electrode，gassensorsandmagneticmaterialsPreparationandapplicationsofNiON

2、anopowdersarereViewedanywhereThereareawideVa“etyofpreparations01utionsofNiONano。powdersTherefore，itisimportanttochooseapreparationsolutionwhichhassuchadVantagesassimpletechniques，10wcostandeasytobeindustrializedandscient

3、ificparametersTheauthorcarriesoutanexperimenttoprepareNiONano‘powderscontainingdiffbrentnickelsaltsandprecipitationagentsvialiquidchemicalprecipitationAntimony—dopedtinoxide(ATO)isanimportantmemberoftransparentconductiVe

4、oxidesThepreparationandapplicationofthenanometertransparentandconductiVematerialswaspaidmoreattentionintheabroad，especiallyAme“canandJapanHoweVerinourcountryitmainlydependsontheimportedproductThisexperiment’stargetisimpr

5、oVetheproduct’characters，andtakeplaceoftheimportedproduct√氣TOparticleshaVebeensynthesizedbysolidstatereaction，co。precipitationandhydrothermalmethodsThemajordisadvantagesofthesepreparationmethodsarelargerparticlesize，impu

6、rityinductionandhighcostInthispaper，itissigni行canceforexploringanewpreparationofconductiveATonanoparticles1TheNiCl2‘6H20andNiS046H20werechosenasnickelsaltsNa2C03，NaoH，NH3’H20andH2C204。2H20asprecipitationagents，preparingd

7、iff色renttopographyNiONano—powdersViasinglephaseprecipitationTheprecursorhasbeendetectedbyDSC／TGThestructure，particlesizesandtopographyofNiOpowderswereinVestigatedbymeansofXRDandSEMTheresultsoftheDSC／TGshowthattheprecurso

8、rwascompletelydecomposedunder400℃TheresultsoftheXRDshowthatNiONanopowderswerecubecrystalstructureThediffractionpeakswerein3730，4330and6290，whichwereconsistentwithnomalpatternTheresultsoftheSEMshowthatthewaycomesoutfirstw

9、echooseNiS04asnickelsalt，NH3。H20andH2C204‘2H20asprecipitationagentsviasinglephaseprecipitationTheoptimumparametersweredeteminedinthissystemas：pHvaluesofsolution84，reactiontemperature60℃，concentrationofNi2O8mol／L，roasting